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Present data
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Reference data [33]
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|---|
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Position
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δC (ppm)
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δH (ppm)
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δC (ppm)
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δH (ppm)
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|---|
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1
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151.49
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–
|
150.2
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–
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|
2
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124.73
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–
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125.2
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–
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3
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133.30
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–
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132.8
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–
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4
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119.58
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7.12 (1H, s)
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119.4
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7.21 (1H, s)
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5
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122.58
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7.40 (1H, dd, J = 1.3, 8.2 Hz)
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122.3
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7.47 (1H, dd, J = 1.0, 8.0 Hz)
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6
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127.20
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7.36 (1H, d, J = 8.2 Hz)
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127.3
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7.40 (1H, dd, J = 8.0, 8.0 Hz)
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7
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110.51
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7.28 (1H, dd, J = 1.3, 7.3, Hz)
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110.7
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7.30 (1H, dd, J = 1.0, 8.0 Hz)
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|
8
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154.71
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–
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154.2
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–
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9
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113.54
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–
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113.2
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–
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10
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136.74
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–
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135.7
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–
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1′
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102.84
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5.05 (1H, d, J = 7.9 Hz)
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102.6
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5.04 (1H, d, J = 7.5 Hz)
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2′
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73.57
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3.46 (1H, t, J = 8.8 Hz)
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73.3
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3.39 (1H, m)
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|
3′
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76.82
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3.37 (1H, m)
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76.2
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3.36 (1H, m)
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4′
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70.13
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2.91 (1H, m)
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70.1
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3.18 (1H, m)
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|
5′
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76.10
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3.68 (1H, m)
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76.0
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3.59 (1H, m)
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|
6′
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66.59
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4.05 ( 1H, d, J = 8.9 Hz); 3.63 (1H, m)
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66.6
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3.93 (1H, dd, J = 1.5, 11.0 Hz); 3.50 (2H, m)
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|
1′′
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100.86
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4.71 (1H, d, J = 1.4 Hz)
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100.7
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4.62 (1H, d, J = 1.5 Hz)
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2′′
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70.84
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3.84 (1H, dd, J = 1.6, 3.4 Hz)
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70.4
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3.68 (1H, m)
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3′′
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71.03
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3.63 (1H, m)
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70.7
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3.50 (2H, m)
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4′′
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72.59
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3.31 (1H, m)
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71.9
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3.20 (1H, m)
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5′′
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68.55
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3.52 (1H, m)
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68.4
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3.49 (1H, m)
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6′′
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16.55
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1.17 (3H, d, J = 6.2 Hz)
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17.7
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1.12 (3H, d, J = 6.0 Hz)
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|
ArCH3
|
18.49
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2.25 (3H, s)
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19.0
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2.25 (3H, s)
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|
COCH3
|
41.3
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2.97 (3H, s)
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31.9
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2.52 (3H, s)
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|
COCH3
|
207.07
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–
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204.4
|
–
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- s, singlet, d, doublet, dd, doublet of doublets, m, multiplet, br, broad, t, triplet
